1. Universidade Federal da Bahia
  2. Escola Politécnica
  3. Programa de Pós-graduação em Engenharia Civil (PPEC)
  4. Tese (PPEC)
Use este identificador para citar ou linkar para este item: https://repositorio.ufba.br/handle/ri/38759
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Campo DCValorIdioma
dc.creatorCosta, Ana Rita Damasceno-
dc.date.accessioned2023-12-21T13:57:11Z-
dc.date.available2023-12-21T13:57:11Z-
dc.date.issued2023-10-27-
dc.identifier.urihttps://repositorio.ufba.br/handle/ri/38759-
dc.description.abstractThe valorisation of industrial residues or by-products in the production of Portland clinker is a promising alternative for developing sustainable cements. The complexity of chemical reactions during clinkering requires an appropriate dosing method that considers the effect of impurities in raw materials to maximise the potential substitution of natural resources with residues or by-products, while ensuring the reactivity requirements of clinker. This study investigated the effect of impurities from co-processed alternative raw materials on the production of ordinary and alternative Portland clinkers using thermodynamic modelling. In the first step, a dosing and optimisation method for raw meals was developed using thermodynamic modelling to facilitate the co-processing of alumina-rich residues and maximise the reactivity of Portland clinker. Then, this method was applied to co-process the spent fluid catalytic cracking catalyst (SFCC), focusing on experimentally evaluating the effect of its impurities on the clinker. In the third step, modelling was used to investigate the effect of some of the main impurities of SFCC (lanthanides) on clinker production. Subsequently, the study evaluated the effect of alkali metals on the manufacture of belite clinker using thermodynamic modelling validated with experimental data from the literature. Lastly, the influence of co-processed SFCC on high ferrite Portland clinker (HFPC) was investigated. The proposed dosing method optimised the composition of the raw meal, resulting in clinkers with higher amounts of tricalcium silicate (potentially more reactive) and limited tricalcium aluminate content. The dosed samples produced clinkers with more than 50% Ca5SiO3, even when 15% SFCC was co-processed in the raw meal. The optimised chemical combination of the impurities, the maximisation of cement reactivity, the reduction of natural limestone and clay consumption, and the proper disposal of SFCC are positive implications of the proposed method for clinker dosing. Thermodynamic modelling demonstrated that the co-processing of lanthanides promoted the formation of new compounds, mainly cubic perovskite containing Al and O. However, Ce2O3 remained in its pure crystalline forms. Increased lanthanide content generally stabilised calcium aluminoferrite, suggesting that these elements could be used to produce cements with high ferrite content (8~20%) and resistance to sulfate attack. Thermodynamic calculations simulated the formation reactions of belite clinker and confirmed the findings of previous experimental studies. In the presence of sodium (Na) doping, Ca3(Al,Fe)O6 was destabilised, resulting in orthorhombic tricalcium aluminate and minor phases. Potassium (K) doping increased Ca2(Al,Fe)O5 and potassium silicates as minor phases. The thermodynamic modelling of SFCC co-processing in HFPC differed from the experimental results for the CaO-Al2O3-Fe2O3 phases, mainly due to the simulation of new compounds containing dopants non-quantified by the experimental method. Thermodynamic modelling enhanced the understanding of phase evolution, the stabilisation of calcium aluminoferrite solutions, changes in the melt phase viscosity, and the volume of phases during the simulations. This technique proved to be an important tool for optimising industrial processes and environmentally safe production of clinkers containing residual raw materials.pt_BR
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado da Bahia (FAPESB)pt_BR
dc.languageporpt_BR
dc.publisherUniversidade Federal da Bahiapt_BR
dc.rightsAttribution-NonCommercial-NoDerivs 3.0 Brazil*
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/3.0/br/*
dc.subjectModelagem termodinâmicapt_BR
dc.subjectClínquerpt_BR
dc.subjectCoprocessamentopt_BR
dc.subjectMétodo de dosagempt_BR
dc.subjectCimentopt_BR
dc.subjectImpurezaspt_BR
dc.subjectGestão de resíduospt_BR
dc.subject.otherThermodynamic modellingpt_BR
dc.subject.otherClinkerpt_BR
dc.subject.otherCoprocessingpt_BR
dc.subject.otherDosing methodpt_BR
dc.subject.otherCementpt_BR
dc.subject.otherImpuritiespt_BR
dc.subject.otherWaste managementpt_BR
dc.titleAplicação da modelagem termodinâmica da clinquerização para dosagem e coprocessamento de matérias-primas na produção de cimentospt_BR
dc.typeTesept_BR
dc.publisher.programPrograma de Pós-graduação em Engenharia Civil (PPEC) pt_BR
dc.publisher.initialsUFBApt_BR
dc.publisher.countryBrasilpt_BR
dc.subject.cnpqCNPQ::ENGENHARIASpt_BR
dc.subject.cnpqCNPQ::ENGENHARIAS::ENGENHARIA CIVIL::CONSTRUCAO CIVIL::MATERIAIS E COMPONENTES DE CONSTRUCAOpt_BR
dc.contributor.advisor1Gonçalves, Jardel Pereira-
dc.contributor.advisor1IDhttps://orcid.org/0000-0003-3484-3869pt_BR
dc.contributor.advisor1Latteshttp://lattes.cnpq.br/5363080225273626pt_BR
dc.contributor.advisor-co1Kirchheim, Ana Paula-
dc.contributor.advisor-co1IDhttps://orcid.org/0000-0002-8241-0331pt_BR
dc.contributor.advisor-co1Latteshttp://lattes.cnpq.br/4014435019322019pt_BR
dc.contributor.referee1Albuquerque, Elaine Christine de Magalhães Cabral-
dc.contributor.referee1IDhttps://orcid.org/0000-0002-3472-9129pt_BR
dc.contributor.referee1Latteshttp://lattes.cnpq.br/1624091546521389pt_BR
dc.contributor.referee2Martínez, Erich David Rodríguez-
dc.contributor.referee2IDhttps://orcid.org/0000-0003-1914-4541pt_BR
dc.contributor.referee2Latteshttp://lattes.cnpq.br/6109846594507875pt_BR
dc.contributor.referee3Pontes, Karen Valverde-
dc.contributor.referee3IDhttps://orcid.org/0000-0002-8208-0854pt_BR
dc.contributor.referee3Latteshttp://lattes.cnpq.br/5444380855577045pt_BR
dc.contributor.referee4Fiuza Junior, Raildo Alves-
dc.contributor.referee4IDhttps://orcid.org/0000-0001-8235-6876pt_BR
dc.contributor.referee4Latteshttp://lattes.cnpq.br/0513144318630937pt_BR
dc.contributor.referee5Bielefeldt, Wagner Viana-
dc.contributor.referee5IDhttps://orcid.org/0000-0003-3984-7703pt_BR
dc.contributor.referee5Latteshttp://lattes.cnpq.br/2314494393454115pt_BR
dc.creator.IDhttps://orcid.org/0000-0001-8526-0036pt_BR
dc.creator.Latteshttp://lattes.cnpq.br/7390168408894641pt_BR
dc.description.resumoA valorização de resíduos ou subprodutos industriais na produção do clínquer Portland é uma alternativa promissora para o desenvolvimento de cimentos sustentáveis. A complexidade das transformações e reações químicas durante a clinquerização exige um método de dosagem de insumos adequado que considere o efeito das impurezas para maximizar a potencial substituição de recursos naturais por resíduos ou subprodutos, garantindo os requisitos de reatividade do clínquer. Este estudo investigou o efeito de impurezas de matérias-primas alternativas coprocessadas na produção do clínquer Portland convencional e alternativos aplicando modelagem termodinâmica. Na primeira etapa foi desenvolvido um método de dosagem e otimização da farinha crua por modelagem termodinâmica visando o coprocessamento de resíduos ricos em alumina e a maximização da reatividade do clínquer Portland. Em seguida, o método foi aplicado para coprocessar o resíduo de catalisador de craqueamento catalítico (SFCC), avaliando-se experimentalmente o efeito das suas impurezas no clínquer. Na terceira etapa, a modelagem foi utilizada para investigar o efeito de algumas das principais impurezas do SFCC (lantanídeos) na produção do clínquer. A etapa seguinte avaliou o efeito de metais alcalinos na fabricação do clínquer belítico utilizando a modelagem termodinâmica validada com dados experimentais da literatura. A última etapa investigou a influência do SFCC coprocessado no clínquer Portland rico em ferrita (HFPC). O método de dosagem proposto otimizou a composição das farinhas, promovendo clínqueres com mais silicato tricálcico (potencialmente mais reativos) e limitando o teor de aluminato tricálcico. As amostras dosadas produziram clínqueres com mais de 50% de Ca5SiO3, mesmo quando 15% de SFCC foi coprocessado na farinha crua. A otimização da combinação química das impurezas do resíduo, a maximização da reatividade do cimento, a redução do consumo de calcário e argila naturais e a destinação adequada do SFCC são implicações positivas do método proposto para a dosagem do clínquer. A modelagem termodinâmica demonstrou que o coprocessamento de lantanídeos promoveu a formação de novos compostos, principalmente a perovskita cúbica contendo Al e O. No entanto, o Ce2O3 permaneceu em suas formas cristalinas puras. O aumento do teor de lantanídeos geralmente estabilizou cálcio aluminoferrita, sugerindo que esses elementos podem ser aplicáveis para produzir cimentos com alto teor de ferrita (8~20%) e resistentes ao ataque por sulfatos. Os cálculos termodinâmicos permitiram simular as reações de formação do clínquer belítico e corroboraram os resultados experimentais prévios. O Ca3(Al,Fe)O6 foi desestabilizado no clínquer dopado com Na, resultando em aluminato tricálcico ortorrômbico e fases minoritárias. Para amostras dopadas com K, observou-se o aumento do Ca2(Al,Fe)O5 e silicatos de potássio como fases minoritárias. A modelagem do coprocessamento do SFCC no HFPC diferiu dos resultados experimentais para as fases CaO-Al2O3-Fe2O3, principalmente devido à simulação de novos compostos contendo dopantes não quantificados pelo método experimental. A modelagem termodinâmica ampliou o entendimento sobre a evolução das fases, a estabilização das soluções de cálcio aluminoferrita, mudanças na viscosidade da fase fundida e no volume das fases ao longo das simulações. A técnica demonstrou ser uma ferramenta importante para otimizar processos industriais e a produção ambientalmente segura de clínqueres contendo matérias-primas residuais.pt_BR
dc.publisher.departmentEscola Politécnicapt_BR
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